Preparation of titanium (III) coordination complexes

Details Preparation of titanium (III) coordination complexes Preparation of titanium (III) coordination complexes

1993-04-01

1993-11-23

Dees, Jose G.

Organic compounds -- part of the class 532-570 series

Organic compounds

Heterocyclic carbon compounds containing a hetero ring...

549210, 556 54, 556 56, C07D49312, C07F 728

Patent

active

052645908

ABSTRACT:
Ti(III) coordination complexes with ethers are prepared by the steps of (a) forming an ether complex of a Ti(IV) salt by adding a stoichiometric excess of an ether to said salt, and then (b) reducing said complex with an organometallic reducing agent such as an aluminum alkyl or a lithium compound to form a Ti(III)-ether coordination complex.

REFERENCES:
patent: 3769233 (1973-10-01), Hermans et al.
patent: 4210736 (1980-07-01), Baekelmans et al.
Fowles et al., J. Chem. Soc., pp. 5873-5878 (1963).
Clark et al., J. Chem. Soc., pp. 379-387 (1963).

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