Preparation of mono epoxides and tertiary butyl alcohol using re

Details Preparation of mono epoxides and tertiary butyl alcohol using re Preparation of mono epoxides and tertiary butyl alcohol using re

1992-08-24

1993-06-01

Evans, Joseph E.

Harness for working animal

502 24, 502 33, 5089098, C07D30114, C07D30304

Patent

active

052161820

ABSTRACT:
In the preparation of tertiary butyl alcohol and a linear C.sub.3 -C.sub.12 mono epoxide by the epoxidation reaction of a linear C.sub.3 -C.sub.12 alpha mono olefin with tertiary butyl hydroperoxide in solution in tertiary butyl alcohol in the presence of a catalytic amount of a soluble complex of molybdenum with ethylene glycol, a portion of the catalyst that is used is a recycle (final) ethylene glycol solution of a complex of ethylene glycol with ammonium-containing molybdenum compounds prepared from ethylene glycol and a precipitate of solid ammonium-containing molybdenum compounds formed by saturating a heavy distillation fraction with ammonia to thereby form a liquid amination product containing a precipitate of solid ammonium-containing molybdenum compounds; the heavy distillation fraction being obtained by distillation of the epoxidation reaction product.

REFERENCES:
patent: 3931044 (1976-01-01), Maurin
patent: 4598057 (1986-07-01), Isaacs
patent: 4626596 (1986-12-01), Marquis et al.
patent: 5101052 (1992-03-01), Meyer et al.
patent: 5107067 (1992-04-01), Marquis et al.

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