Chemistry of carbon compounds – Miscellaneous organic carbon compounds – C-metal
Patent
1978-02-27
1979-04-03
Sebastian, Leland A.
Chemistry of carbon compounds
Miscellaneous organic carbon compounds
C-metal
C07C 7912
Patent
active
041477324
ABSTRACT:
An improvement is disclosed in the preparation of pentachloronitrobenzene by the nitration of pentachlorobenzene. The improvement, which is primarily aimed at reducing the residual level of the undesirable starting material, pentachlorobenzene, in the product, includes a two-stage reactant mixing step wherein the pentachlorobenzene is first mixed with sulfuric acid and then concentrated nitric acid is added to this mixture.
REFERENCES:
patent: 3026358 (1962-03-01), Lojewski
patent: 3984487 (1976-10-01), Watts, Jr. et al.
patent: 4026955 (1977-05-01), Breaux et al.
patent: 4057950 (1977-11-01), Gay
O'Day Thomas P.
Olin Corporation
Sebastian Leland A.
Simons William A.
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