Process for producing 4-carbamoyl-1H-imidazolium-5-olate

Organic compounds -- part of the class 532-570 series – Organic compounds – Heterocyclic carbon compounds containing a hetero ring...

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C07D23370

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active

045032351

ABSTRACT:
A process is provided for producing 4-carbamoyl-1H-imidazolium-5-olate (I) ##STR1## by reacting aminomalonamide H.sub.2 N--CH(CONH.sub.2).sub.2 and formamidine CH(.dbd.NH)NH.sub.2 compound in a liquid medium comprising alcohol under conditions such that the product I can be obtained in a solid form that is directly recoverable from the medium, free of aminomalonamide and recrystallizable.

REFERENCES:
patent: 4218457 (1980-08-01), Atsumi et al.
Schipper and Day, J. Am. Chem. Soc., 74, pp. 350-353, 1952.

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