Polymerization of aniline and its derivatives

Chemistry: electrical and wave energy – Processes and products

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204 59R, 204 72, 528422, C25B 302

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active

049405179

ABSTRACT:
Electrically conductive polyaniline and its derivatives are prepared by polymerizing compounds of the Formula: ##STR1## wherein R is --H, --OH, lower alkoxy, halogen, --COOH, --NO.sub.2 or --NH.sub.2 ; x is 0 to 4, with substitutions being ortho or meta to the amine group; R' is hydrogen or lower alkyl; comprising reacting the compound of Formula I with an initiator in the presence of a chemical oxidant and/or an applied electrochemical potential, said initiator comprising a substituted or unsubstituted aromatic amine which has a lower oxidation potential than the compound of Formula I, and which is capable of being incorporated into the polymer chain resulting from the polymerization reaction.

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Walter W. Focke et al., "Influence of Oxidation State, pH, and Counterion on the Conductivity of Polyaniline," J. Phys. Chem., 91:5813 (1987).
Akira Kitani et al., "A Conducting Polymer Derived from Para-Aminodiphenylamine," J. Electroanal. Chem. 221:69 (1987).

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