Compound: d-N-(2-amino-2-phenethyl)-2-methoxyethylamine and proc

Details Compound: d-N-(2-amino-2-phenethyl)-2-methoxyethylamine and proc Compound: d-N-(2-amino-2-phenethyl)-2-methoxyethylamine and proc

1978-11-06

1983-01-25

Hines, Robert V.

Organic compounds -- part of the class 532-570 series

Organic compounds

Amino nitrogen containing

26050117, 564372, C07C 8728

Patent

active

043705006

ABSTRACT:
There is provided a new compound: d-N-(2-amino-2-phenethyl-2-methoxyethylamine useful in the direct synthesis of levamisole. The compound is prepared by slurrying the racemic N-(2-amino-2-phenethyl)-2-methoxyethylamine with dibenzoyl-d-tartaric acid as the resolving agent in an aqueous acidic menstruum containing ammonium chloride, heating the resultant mixture, preferably under reflux, cooling and filtering the resultant mixture to recover crystals rich in the desired d-amine compound, hereinabove noted.

REFERENCES:
patent: 3312733 (1967-04-01), Howe
patent: 3478101 (1969-11-01), Tsuruga et al.
patent: 3819689 (1974-06-01), Thompson et al.
patent: 3845070 (1974-10-01), McMenim et al.
patent: 3847991 (1974-11-01), Bernardi et al.
patent: 3865836 (1975-02-01), Van Gelder et al.
patent: 3887617 (1975-06-01), Seebach et al.

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