Essentially pure/colorless P.sub.2 NOCl.sub.5

Chemistry of inorganic compounds – Phosphorus or compound thereof – Halogen containing

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423302, 423304, 423386, 423462, C01B 2510

Patent

active

049024906

ABSTRACT:
Essentially pure and colorless N-(dichlorophosphoryl)trichlorophosphazene [P.sub.2 NOCl.sub.5 ] is prepared/purified under relatively moderate conditions, by reacting phosphorous pentachloride with ammonium chloride, treating the resulting medium of reaction, containing P.sub.3 NCl.sub.12, with SO.sub.2, and thin film evaporating the medium of reaction, advantageously in two stages, to eliminate SO.sub.2, POCl.sub.3 and SOCl.sub.2 values therefrom.

REFERENCES:
patent: 1356878 (1920-10-01), Newton
patent: 2925320 (1960-02-01), Kahler
patent: 3231327 (1966-01-01), Seglin et al.

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