Process for stabilizing aqueous solutions of acetoacetamides wit

Details Process for stabilizing aqueous solutions of acetoacetamides wit Process for stabilizing aqueous solutions of acetoacetamides wit

1984-09-10

1986-02-18

Shaver, Paul F.

Organic compounds -- part of the class 532-570 series

Organic compounds

Amino nitrogen containing

C07C10200, C07C103147

Patent

active

045714339

ABSTRACT:
A process for stabilizing aqueous solutions of acetoacetamides which simultaneously results in the reduction of .beta.-aminocrotonic acid amide content. According to the process, to aqueous acetoacetamide solutions which have been prepared in a known manner by the reaction of diketene with ammonia or water-soluble primary or secondary aliphatic amines under basic conditions, sufficient amounts of diketene are added immediately after their preparation thereto at room temperature with vigorous stirring, to maintain a pH value of 6-7. The so obtained aqueous solutions of the acetoacetamides are not only substantially stable, but also especially pure since these solutions are neither contaminated by salt-like by-products nor by derivatives of .beta.-aminocrotonic acid amides.

REFERENCES:
patent: 2863918 (1958-12-01), Bikales et al.

Affiliated with

Also associated with

Rating

Process for stabilizing aqueous solutions of acetoacetamides wit does not yet have a rating. At this time, there are no reviews or comments for this patent.

If you have personal experience with Process for stabilizing aqueous solutions of acetoacetamides wit, we encourage you to share that experience with our LandOfFree.com community. Your opinion is very important and Process for stabilizing aqueous solutions of acetoacetamides wit will most certainly appreciate the feedback.

Rate now

Comments { 0 }

Profile ID: LFUS-PAI-O-1551238