Chemistry of carbon compounds – Miscellaneous organic carbon compounds – C-metal
Patent
1972-10-25
1976-07-06
Myers, Jane S.
Chemistry of carbon compounds
Miscellaneous organic carbon compounds
C-metal
260383, 260384, C07C 7937
Patent
active
039681300
ABSTRACT:
The invention relates to a process for the manufacture of anthraquinones which are mononitrated in the .alpha.-position, especially 1-nitroanthraquinone, wherein an anthraquinone which possesses at least 1 free .alpha.-position and is optionally substituted in the other .alpha.-position with halogen, preferably chlorine, or with hydroxyl groups, but especially the unsubstituted anthraquinone, is nitrated with concentrated nitric acid without further additives adiabatically, or at temperature above 40.degree.C isothermically, and optionally under pressure.
REFERENCES:
patent: 2302729 (1942-11-01), Whelen
patent: 2874168 (1959-02-01), Graham et al.
patent: 3798243 (1974-03-01), Toth
Beisler et al., J.A.C.S. 44 pp. 2298-2303 (1944).
Reichel et al., as cited in CA. 70, 38877z (1969).
Almaula Prabodh I.
Ciba-Geigy AG
Kolodny Joseph G.
McC. Roberts Edward
Myers Jane S.
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