Process of reducing higher metal oxides to lower metal oxides

Details Process of reducing higher metal oxides to lower metal oxides Process of reducing higher metal oxides to lower metal oxides

1986-11-13

1988-12-06

McFarlane, Anthony

Chemistry of inorganic compounds

Treating mixture to obtain metal containing compound

Group viib metal

423148, 423592, 423605, 423632, 75 26, 75 35, 75 36, 75 82, 75 91, C01G 4502, C01G 4904

Patent

active

047895802

ABSTRACT:
Disclosed is a process to effect a reduction to a desired, constant degree as exactly as possible and to achieve a low surplus of carbon. The reduction by treatment with carbonaceous reducing agents is effected in such a manner that fine-grained solids, which contain higher metal oxides, are calcined at 800.degree. to 1100.degree. C. with hot gases in which the solids are suspended. The calcined solids are reduced at a temperature in the range of from 800.degree. to 1100.degree. C. to form low metal oxides in a stationary fluidized bed, which is supplied with carbonaceous reducing agents and oxygen-containing gases. The carbonaceous reducing agents are supplied to the stationary fluidized bed at such a rate so as to reduce the higher metal oxides to low metal oxides, while maintaining the reduction temperature in the stationary fluidized bed and insuring that the discharged matter has the desired carbon content. The stationary fluidized bed exhaust gas is supplied as secondary gas to the calcining step, and fuel is supplied to the calcining step at a rate such that the total of the heat generated by the combustion of the fuel and of the heat suplied by the exhaust gas provides the heat which is required for calcination.

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