Process for preparing 3-azabicyclo(3.1.0)hexane-2-carboxylic aci

Details Process for preparing 3-azabicyclo(3.1.0)hexane-2-carboxylic aci Process for preparing 3-azabicyclo(3.1.0)hexane-2-carboxylic aci

1979-06-18

1981-03-10

Tovar, Jose

Chemistry of carbon compounds

Miscellaneous organic carbon compounds

C-metal

C07D20720, C07D20722

Patent

active

042553342

ABSTRACT:
3-Azabicyclo(3.1.0)hexane-2-carboxylic acid, a plant gametocide, is prepared by effecting reaction between cis 2-aminomethylcyclopropyl-1,1-dimethyl acetal and a cyanide in the presence of a liquid lower-alkanecarboxylic acid; treating the resulting N-alkanoyl-3-azabicyclo(2.1.0)hexane-2-carbonitrile with a strong acid; treating the resulting 3-alkanoyl-3-azabicyclo(3.1.0)hexane-2-carboxylic acid with strong acid to form the desired 3-azabicyclo(3.1.0)hexane-2-carboxylic acid.

REFERENCES:
patent: 4047930 (1977-09-01), Kerr

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