Chemistry of inorganic compounds – Phosphorus or compound thereof – Oxygen containing
Patent
1976-03-17
1977-04-12
Peters, G. O.
Chemistry of inorganic compounds
Phosphorus or compound thereof
Oxygen containing
423305, 71 43, C01B 1516, C01B 2526
Patent
active
040175898
ABSTRACT:
Ammonium polyphosphates are prepared by a process which comprises heating melamine orthophosphate prepared from impure wet-process phosphoric acid in a stream of gaseous ammonia at a temperature between 150.degree. C and 210.degree. C to produce a mixture of melamine and relatively pure short-chain ammonium polyphosphates. The solid product is extracted with water to remove the ammonium polyphosphates and free the insoluble, crystalline melamine for recycle. Thus, the only starting materials consumed in the process are phosphoric acid and ammonia.
REFERENCES:
patent: 3912802 (1975-10-01), McCullough et al.
patent: 3920796 (1975-11-01), Sheridan
T921,024, May 1974, Sheridan, 423/305.
T904,031 Nov. 1972, McCullough et al., 423/305.
McCullough John F.
Sheridan Richard C.
Heller Gregory A.
Peters G. O.
Petrusek Robert A.
Tennessee Valley Authority
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