Process for preparing solutions of N-methylol-chloroacetamide

Details Process for preparing solutions of N-methylol-chloroacetamide Process for preparing solutions of N-methylol-chloroacetamide

1976-07-01

1978-02-21

Demers, Arthur P.

Chemistry of carbon compounds

Miscellaneous organic carbon compounds

C-metal

424320, C07C10338

Patent

active

040752453

ABSTRACT:
Higly concentrated solutions of N-methylol-chloroacetamide are prepared by treating chloracetic acid methyl ester in solution in isopropanol with ammonia at temperatures of -20.degree. to 10.degree. C and then reacting with paraformaldehyde at temperatures of 60.degree. to 120.degree. C after the addition of water and a basic catalyst.

REFERENCES:
Vail et al., J. Org. Chem. 27 (1962) p. 2067-2070.
Wagner et al., Synthetic Organic Chemistry, John Wiley & Sons, N.Y., 1955 pp. 568-569.

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