Process for preparation of quinacridone pigments using moderatel

Organic compounds -- part of the class 532-570 series – Organic compounds – Heterocyclic carbon compounds containing a hetero ring...

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546 56, 546 57, 106288Q, C09B 4800

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active

042476950

ABSTRACT:
A process for preparing beta or gamma crystals of linear quinacridone, substituted quinacridone or solid solutions thereof by contacting premilled quinacridone with 45-60% by weight sulfuric acid and 0-10% by weight of a surfactant based on the quinacridone at a weight ratio of acid to quinacridone of 3:1-6:1 to form a slurry, agitating said slurry for a period of time at 45.degree.-75.degree. C., adding water to form a dilute slurry, agitating said dilute slurry for a period of time at 75.degree.-95.degree. C. and separating quinacridone from the liquid of the dilute slurry.

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patent: 4088506 (1978-05-01), Wetzel
patent: 4094699 (1978-06-01), Fitzgerald
Takagi, et al., Chemical Abstracts, vol. 77, 128029Y (1972).

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