Method for producing C.sub.1 to C.sub.5 alkyl nitrides

Details Method for producing C.sub.1 to C.sub.5 alkyl nitrides Method for producing C.sub.1 to C.sub.5 alkyl nitrides

1989-12-05

1990-12-25

Maples, John S.

Organic compounds -- part of the class 532-570 series

Organic compounds

Nitrite esters or chalcogen analogues thereof

C07C20108

Patent

active

049804960

ABSTRACT:
The invention provides a process for the production of C.sub.1 to C.sub.5 alkyl nitrite by forming an aqueous solution of C.sub.1 to C.sub.5 alkyl alcohol an alkali metal nitrite; cooling it; then slowly adding a hydrohalic acid solution while it is stirring; the reaction temperature is maintained in the range of from about -10.degree. C. to about 10.degree. C. until the reaction is substantially complete; and the two formed phases are separated in a separatory funnel.

REFERENCES:
patent: 2166698 (1939-07-01), Allen
patent: 2465984 (1946-05-01), Doumani et al.
patent: 2739166 (1956-03-01), Treacy
patent: 2831882 (1958-04-01), Spaeth
patent: 3214458 (1965-10-01), De Rooij et al.
patent: 4353843 (1982-10-01), Doumaux, Jr. et al.
patent: 4908466 (1990-03-01), Nelson
Organic Synthesis Collection; vol. 2, 108 (1943), N-Butyl Nitrite.
Organic Synthesis Collection; vol. 3, 191 (1955), Omega-Chloronitrosoacetophenone.
Chemical Abstracts, 1964, No. 4090, Nitrites.
Chemical Abstracts, 1958, No. 15565, Nitrite Esters.
Chemical Abstracts, 1944, No. 5809, Omega-Chloroisonitrosoacetophenone.
Chemical Abstracts, vol. 30, No. 811, Isopropyl Nitrite.
Chemical Abstracts CA110(17): 153420b.
Chemical Abstracts CA100(17): 138331y.
Chemical Abstracts CA 98(11): 88649a.
Chemical Abstracts CA90(8): 64324z.
Chemical Abstracts CA89(4): 26345d.
Chemical Abstracts CA88(4) 24132n.
Chemical Abstracts CA83(2): 12838p.
Chemical Abstracts CA82(15): 97460d.
Chemical Abstracts CA81(1): 3281a.
Chemical Abstracts CA76(21): 126097z.
Chemical Abstracts CA74(9): 41808r.
Chemical Abstracts CA68(2): 6886u.

Affiliated with

Also associated with

Rating

Method for producing C.sub.1 to C.sub.5 alkyl nitrides does not yet have a rating. At this time, there are no reviews or comments for this patent.

If you have personal experience with Method for producing C.sub.1 to C.sub.5 alkyl nitrides, we encourage you to share that experience with our LandOfFree.com community. Your opinion is very important and Method for producing C.sub.1 to C.sub.5 alkyl nitrides will most certainly appreciate the feedback.

Rate now

Comments { 0 }

Profile ID: LFUS-PAI-O-1164175