Zirconium halohydride preparation

Details Zirconium halohydride preparation Zirconium halohydride preparation

1977-05-02

1979-04-03

Sneed, Helen M. S.

Chemistry of carbon compounds

Miscellaneous organic carbon compounds

C-metal

C07F 700

Patent

active

041477090

ABSTRACT:
Zirconium halohydrides having the formula ##STR1## WHEREIN R is a .pi.-cyclopentadienyl radical are prepared by reacting a dihalide having the formula ##STR2## WITH MOLECULAR HYDROGEN IN THE PRESENCE OF AN UNREACTED Group Ia metal in a solvent for the dihalide.

REFERENCES:
wailes et al., J. Organometal. Chem. 24 405-411 (1970); 28 91-95 (1971).
Hart et al., J.A.C.S. 96 8115-8116 (1974).
Emeleus, Adv. in Inorganic Chem. & Radiochem., Academic Press, N.Y. V7, pp. 116-118 (1965).
Candlin et al., Reactions of Transition-Metal Complexes, Elsevier Publ. Co., N.Y., pp. 328-330 (1968).

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