Zearalanone-zearalanol product

Details Zearalanone-zearalanol product Zearalanone-zearalanol product

1974-02-05

1976-06-01

Patten, James A.

Chemistry of carbon compounds

Miscellaneous organic carbon compounds

C-metal

C07D31300

Patent

active

039608980

ABSTRACT:
The high-melting diastereoisomer of zearalanol or derivative thereof is prepared by heating its corresponding low-melting diastereoisomer under dehydrogenating conditions in the presence of a Raney nickel catalyst and under an oxygen-free atmosphere, and then subjecting the solution to reducing conditions under a hydrogen atmosphere at elevated pressure.

REFERENCES:
patent: 3818044 (1974-06-01), Young
patent: 3839364 (1974-10-01), Young
Kleiderer et al., J. Org. Chem., Vol. 13, (1948), p. 455.

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