Working up reaction mixtures obtained in addition reactions with

Distillation: processes – separatory – With chemical reaction – Including step of adding catalyst or reacting material

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203 63, 203 64, 203 89, 159 49, 568693, B01D 334

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active

056835558

ABSTRACT:
Reaction mixtures obtained in addition reactions of OH-- or NH-- carrying compounds with acetylene or propyne in the presence of alkali metal alcoholates or alkali metal amides are worked up by distilling off the vaporizable components from the reaction mixture in a thin-film evaporator. Before removal of the vaporizable components from the reaction mixture, a particularly defined polyether is added thereto.

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patent: 5095154 (1992-03-01), Liu
Research Disclosure, No. 290, Jun. 1988, p. 389, "Distilling organic compounds in the presence . . . ".
Liebigs Ann. Chem. 601 (1956), 81.
Ullmanns Encykopadie der . . . , 4th Ed., Verlag Chem., vol. 19, p. 31 et seq.

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