Wet pulverizing of polysaccharides

Solid material comminution or disintegration – Processes – By operations other than force of contact with solid surface

Reexamination Certificate

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C241S015000, C241S030000

Reexamination Certificate

active

07357339

ABSTRACT:
Polysaccharide is wet pulverized by ejecting a liquid dispersion of polysaccharide from a pair of nozzles under a high pressure of 70 to 250 MPa to form a pair of jets so that the jets collide against each other. The nozzles are oriented to define a collision angle of 95-178° and the number of pulverizing cycles is adjusted such that the polysaccharide is pulverized to an average particle length which is equal to or less than ¼ of the initial average particle length while undergoing a reduction in degree of polymerization of less than 10%.

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Jinping Zhou et al., Solubility of Cellulose in NaOH/Urea Aqueous Solution, Polymer Journal, vol. 32, No. 10, pp. 866-870 (2000).

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