Chemistry: analytical and immunological testing – Process or composition for determination of physical state... – Corrosion resistance or power
Reexamination Certificate
1999-09-20
2004-01-27
Alexander, Lyle A. (Department: 1743)
Chemistry: analytical and immunological testing
Process or composition for determination of physical state...
Corrosion resistance or power
C436S005000, C436S002000, C436S135000, C436S166000, C422S053000, C073S865600
Reexamination Certificate
active
06682932
ABSTRACT:
FIELD OF THE INVENTION
This invention relates to a test method for evaluating weatherability of articles and materials thereof and an apparatus for carrying out the test. More specifically, the invention is applied to a weatherability test of organic materials, articles made of the organic materials, articles coated with the organic materials, and the like which are used outdoors.
BACKGROUND OF THE INVENTION
Weathering tests designed to evaluate weatherability of organic materials such as coatings include an outdoor exposure test in which a test piece is exposed to the weather and a traced and collected sunlight exposure test in which a test piece is exposed to traced and collected sunlight. In addition, special test methods include an artificial accelerated weathering test in which a test piece is irradiated with light from an artificial light source by means of a weathering apparatus, such as a sunshine weather meter, a UV carbon weatherometer, a xenon weatherometer, a dew panel weatherometer, and a metal halide weatherometer.
JP-A-48-60695 discloses a method for accelerating a salt spray test for evaluating anticorrosion of steel stock against seawater, in which hydrogen peroxide-added salt water is used as testing seawater.
The above-mentioned outdoor exposure test and traced and collected sunlight exposure test require an extremely long period of time not shorter than several months for test pieces to be deteriorated. It has been impossible with these weathering tests to evaluate weatherability rapidly.
The problem of the artificial accelerated weathering test, on the other hand, is that the test fails to sufficiently reproduce the deterioration that should have been resulted from exposure to natural weathering conditions. That is, the deteriorated state of a test piece does not agree with that in the outdoors for the following reason. When articles or materials are long-term exposed outdoors, their deteriorated surface, typically the coating film, shows a surface profile with fine waviness and fine pits in a mixed state, both of which reduce the surface gloss, whereas the surface profile developed in the accelerated weathering test mainly displays fine waviness so that the reduction in gloss as observed is chiefly ascribed to the fine waviness alone.
The above-described improved salt spray test aims at acceleration of a durability test, but its application is limited to evaluation of anticorrosion of steel stock against seawater in special fields. It does not apply to weatherability testing of organic materials or articles thereof.
SUMMARY OF THE INVENTION
An object of the present invention is to provide a test method and an apparatus for evaluating weatherability of organic materials, articles made of organic materials, and materials coated with organic materials in an accelerated manner to greatly reduce the testing time.
Another object of the invention is to provide a weathering test method and an apparatus therefor which greatly speed up deterioration of a test piece while achieving satisfactory reproduction of outdoor deterioration.
The invention relates to a weathering test method and a weathering apparatus for evaluating weatherability of a test piece such as an organic material, an article made of an organic material or an article coated with an organic material.
The invention provides in its first aspect a weathering test method comprising making active oxygen and light simultaneously act on a test piece and evaluating the resultant deterioration, and a weathering apparatus used to carry out the test method.
The invention provides in its second aspect a weathering test method comprising successive and/or alternate steps of making active oxygen and light simultaneously act on a test piece and making at least one of light, oxygen, and water to act on the test piece, and a weathering apparatus used to carry out the test method.
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Mori Kanji
Narita Takeshi
Okamoto Kazuo
Tachi Kazuyuki
Tsuji Masao
Alexander Lyle A.
Kabushiki Kaisha Toyota Chuo Kenkyusho
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