Cleaning and liquid contact with solids – Processes – For metallic – siliceous – or calcareous basework – including...
Reexamination Certificate
2000-12-19
2001-08-28
Carrillo, Sharidan (Department: 1745)
Cleaning and liquid contact with solids
Processes
For metallic, siliceous, or calcareous basework, including...
C134S002000, C134S006000, C134S007000, C134S036000, C134S041000, C134S042000, C148S254000, C510S245000, C510S296000, C206S000500, C206S524100, C206S524500, C206S524400, C206S524700
Reexamination Certificate
active
06280528
ABSTRACT:
BACKGROUND OF THE INVENTION
The present invention relates generally to an improved method and/or process for preparing and handling formulations useful in metal treatment baths, and more particularly to a method for preparing and packaging formulations useful in the preparation and replenishing of aqueous-based baths for simultaneously removing soil, grease and oils from metallic surfaces, while at the same time protecting these surfaces against corrosion. The present invention finds particular application in connection with products requiring short and/or intermediate term protection of their metallic surfaces as they are either shipped, stored or otherwise handled while awaiting further operations. Of particular interest is the protection of metallic surfaces of objects such as components, subassemblies and/or weldments which are partially completed in one production operation, and which must await transfer, shipment, and/or other indeterminate storage pending completion of the next operation.
The present invention involves an improved method or process for preparing working solutions of surface treating compounds by pre-blending surface cleaner and corrosion inhibitor components and packaging the resulting blends in water soluble pouches or containers. The method involves packaging water soluble vapor phase corrosion inhibiting chemicals (VCI) in combination with surface cleaners and/or detergents in water soluble pouches or containers so as to permit the addition of these components to baths without the necessity of hand involvement at this step of the process. The water soluble pouches or containers are preferably prepared from polyvinylalcohol (PVA) films, with the highly effective blends of surface cleaner and corrosion inhibiting components being compatible with PVA films, thus providing a significant shelf life for the pouches containing the components to be used in the working solutions.
In manufacturing and/or product processing operations, it has become common practice to manufacture certain components at a first facility or at a first location within a given facility, with the partially completed components being stored and/or held until needed for use in subsequent operations. An example of such a procedure would include a first operation for preparing a formed or configured component, with the component being held in inventory until needed for use and/or treatment in a subsequent operation. The subsequent operation may, for example, be to combine the component with a second component and then undergo the application of a surface coating for the combination. Because of the tendency of certain metallic surfaces to oxidize and/or corrode in the atmosphere, the application of a corrosion inhibitor to the surface is frequently undertaken to retard and/or prevent the creation of oxide layers and/or rust. Thus, in accordance with the present invention, parts prepared at one point in time for use at a later point in time may be cleaned and protected from corrosion and/or rust by treatment in a bath containing a blend of surface cleaners and corrosion inhibitors, with the working solution for the bath being prepared and replenished by the addition of surface cleaners and corrosion inhibitors blended in predetermined proportions and packaged in known quantities in water soluble pouches or containers. The components comprising the working solution may be maintained at their required concentration levels within the bath on an expeditious, effective and safe condition with the water soluble containers that can be added directly to the working solutions.
SUMMARY OF THE INVENTION
The present invention enables the straightforward, simple, and labor-saving method of preparing and replenishing working solutions for protecting metallic surfaces, with the method enabling the addition of cleaning and corrosion inhibiting components directly to the bath with the water soluble containers. Accordingly, the surface cleaning and corrosion inhibiting components for the working solution are initially selected to form a blend compatible with polyvinylalcohol (PVA) films. These selected components are then blended and loaded into the water soluble pouch, with the blending occurring either prior to loading or upon being loaded into the pouch. Thereafter, when its use is indicated, one or more pouches are dropped into the aqueous bath for preparing and/or replenishing the working solution for its intended purpose. Because of the sensitive nature of surface treating chemicals, it is desirable to reduce the episodes and frequency of contact between a worker and the ingredients. Indeed, because of the nature of certain cleaners and corrosion inhibitors, it is generally desirable to avoid and/or reduce skin contact, even though the components selected for use in the present invention are not considered dangerous.
The technique of the present invention is particularly useful in the cleaning stage where the removal of oil, lubricants, cutting fluids, metallic filings and dirt, and the like must be undertaken in order to prepare the metallic parts or components for further treatment or for in-plant storage and/or shipping to a further destination. In accordance with the present invention, selected corrosion inhibitors are added in the chemical formulations for baths or tanks used in metal cleaning or other component preparation operations. Water soluble bags for selected cleaner/corrosion inhibitor blends provides a system useful in maintaining proper processing environment without arbitrary and inaccurate forms of measurement. In addition to providing ease of handling, the bags provide additional safety with elimination of hand contact with chemicals, while at the same time eliminating container disposal problems. Also, the chemicals contained within the bag are all appropriately utilized, without the necessity of weighing operations which are frequently omitted or may not be conveniently available. The components making up the surface cleaner/corrosion inhibitor blends do not react with the water soluble bag, but at the same time, are readily and easily dispersed upon addition to the solutions held in the baths or tanks.
Therefore, it is a primary object of the present invention to provide an improved technique for cleaning and protecting surfaces of metallic components between successive manufacturing operations by cleaning the surfaces and protecting such surfaces against corrosion with a corrosion inhibitor, wherein the technique includes adding predetermined quantities of corrosion inhibitor and surface cleaners to an aqueous bath, with the components being retained within a water soluble container or pouch.
It is a further object of the present invention to package a selected surface cleaner and corrosion inhibitor within a water soluble bag, and thereafter preserving the bag and its contents until use, at which time the bag together with its contents is added directly to a treatment bath.
Other and further objects of the present invention will become apparent to those skilled in the art upon a study of the following specification and appended claims.
DESCRIPTION OF THE PREFERRED EMBODIMENT
In order to effectively practice the present invention, a powdered or liquid mix of surface cleaning and VCI chemical is selected for introduction into a water soluble pouch container, with the shelf life of the blend within the container being limited only by that of the PVA film container. In other words, the components must be selected such that they neither attack nor accelerate any deterioration of the PVA film comprising the container.
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patent: 4973416 (1990-11-01), Kennedy
patent: 5332525 (1994-07-01), Miksic et al.
patent: 5344589 (1994-09-01), Miksic et al.
patent: 5854145 (1998-12-01), Chandler et al.
patent: 6037319 (2000-03-01), Dickler et al.
patent: 6085905 (2000-07-01), Miksic et al.
patent: 6136776 (2000-10-01), Dickler et al.
patent: 6156929 (2000-12-01), Chandler et al.
patent: 0878564 A1 (1998-11-01), None
Cracauer III Clifford
Hobday Michael
Kharshan Margarita
Miksic Boris A.
Carrillo Sharidan
Cortec Corporation
Haugen Law Firm PLLP
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