Vacuum and infra-red radiation solvent evaporation

Distillation: apparatus – Apparatus – Systems

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202206, 202236, 202238, 2022671, 203 2, 203 86, 203 89, 203100, 203DIG22, 159 7, 159 111, 159 112, 159 12, 159 49, 159DIG1, 159DIG7, 159DIG15, 159DIG26, B01D 122, B01D 310, B01D 308

Patent

active

054725755

ABSTRACT:
A rotary evaporator is described utilizing a magnetically driven fluorocarbon cylinder, operating within a solvent container, to create a thin solvent film for rapid evaporation without the usual requirement for rotating the entire solvent container assembly. Infra-red heating is employed for efficient evaporation rates. Solvent heating is controlled during evaporation by a single temperature probe, turning the infra-red heater on and off on demand of the probe. Over heating of the product is prevented by maintaining a solvent residue at or near the conclusion of an evaporation.

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patent: 3091577 (1963-05-01), Pequignot
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patent: 3830698 (1974-08-01), Kleiss
patent: 4790911 (1988-12-01), Parkinson
patent: 4913777 (1990-04-01), Parkinson
patent: 5174864 (1992-12-01), Arbizzani et al.

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