Use of rod mill for initial stage of solder glass grinding

Solid material comminution or disintegration – Processes – Plural successive comminuting operations

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241 30, 241152A, 241170, 241184, 429218, B02C 1720, B02C 1912

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044037422

ABSTRACT:
A dramatic reduction in the time required to fine-grind high borate solder glasses is achieved. In the prior art method, the glass is ball-milled in the presence of an amine for about seven days or more. It has now been discovered that by first rod-milling such glasses for a period of from about 1/2 to about 24 hours, the time required for the "amine grind" can be shortened to a period of from about 1 to 3 days. A further improvement is that rod milling eliminates the laborious sieving procedure previously employed to ensure the absence of undesirably large particles in the feed to the amine grinding operation.

REFERENCES:
patent: 2210357 (1940-08-01), Beament
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patent: 3022017 (1962-02-01), McKenna
patent: 3269668 (1966-08-01), Hall
patent: 3353753 (1967-11-01), Wolfgram
patent: 3486706 (1969-12-01), Weyand
patent: 3521825 (1970-07-01), Morcom
patent: 3917490 (1975-11-01), Brown
"Action in a Rod Mill", Engineering & Mining Journal, vol. 161, No. 3, pp. 82-85.

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