Uncatalyzed liquid phase fluorination of 1230ZA

Organic compounds -- part of the class 532-570 series – Organic compounds – Halogen containing

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C07C 1720

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058773592

ABSTRACT:
An uncatalyzed liquid phase process is provided for the preparation of oligomer free 1233zd via the fluorination of 1230za with a high molar excess of HF. The 1233zd is a known intermediate useful for preparing 245fa.

REFERENCES:
patent: 5616819 (1997-04-01), Boyce et al.

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