Chemistry: physical processes – Physical processes – Crystallization
Patent
1976-01-19
1977-11-01
Emery, Stephen J.
Chemistry: physical processes
Physical processes
Crystallization
23301, 23295R, 127 16, 127 60, 159 17P, 159 44, B01D 902
Patent
active
040563642
ABSTRACT:
A crystallizable solute is crystallized from a solution containing the same by introducing a solution of said solute into a first stage evaporative-crystallization zone together with seed solute crystals. Within the first stage evaporative-crystallization zone the solution is concentrated to yield a saturated first stage concentrate containing crystals of said solute. The crystals of said solute are substantially larger than said seed crystals and are suspended in a solution more concentrated with respect to said solute than the solution supplied to said first evaporative-crystallizaton zone. A stream of said first concentrate is removed from said first evaporative-crystallizaton zone and transferred to a second evaporative-crystallization zone for further concentration or crystallization of solute and for the production of solute crystals of increased size. There is continuously recovered from the second evaporative-crystallization zone a slurry having a total solute or solids content of about 86-94% by weight and containing the solute crystals of desired crystal size.
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Garrett, Industrial and Engineering Chemistry, vol. 53, No. 8, Aug. 1961, pp. 623-628.
Dmitrovsky Morris
Kokke Antoine H.
Amstar Corporation
Emery Stephen J.
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