Two stage continuous crystallization apparatus with controls

Chemistry: physical processes – Physical processes – Crystallization

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23301, 23295R, 127 16, 127 60, 159 17P, 159 44, B01D 902

Patent

active

040563642

ABSTRACT:
A crystallizable solute is crystallized from a solution containing the same by introducing a solution of said solute into a first stage evaporative-crystallization zone together with seed solute crystals. Within the first stage evaporative-crystallization zone the solution is concentrated to yield a saturated first stage concentrate containing crystals of said solute. The crystals of said solute are substantially larger than said seed crystals and are suspended in a solution more concentrated with respect to said solute than the solution supplied to said first evaporative-crystallizaton zone. A stream of said first concentrate is removed from said first evaporative-crystallizaton zone and transferred to a second evaporative-crystallization zone for further concentration or crystallization of solute and for the production of solute crystals of increased size. There is continuously recovered from the second evaporative-crystallization zone a slurry having a total solute or solids content of about 86-94% by weight and containing the solute crystals of desired crystal size.

REFERENCES:
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patent: 3220883 (1965-11-01), Howard
patent: 3261670 (1966-07-01), Chirico
patent: 3530924 (1970-09-01), Domning
patent: 3595624 (1971-07-01), Bradfield
patent: 3622387 (1971-11-01), Grandadam
patent: 3680621 (1972-08-01), Giorgi
patent: 3725127 (1973-04-01), Retali
patent: 3899386 (1975-08-01), Komiyama
patent: 3900292 (1975-08-01), Fairchild
Garrett, Industrial and Engineering Chemistry, vol. 53, No. 8, Aug. 1961, pp. 623-628.

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