Tubular hydrogen permeable metal foil membrane and method of...

Gas separation: apparatus – Apparatus for selective diffusion of gases – Hollow fiber or cylinder

Reexamination Certificate

Rate now

  [ 0.00 ] – not rated yet Voters 0   Comments 0

Details

C095S056000, C096S011000, C029S463000, C029S890044

Reexamination Certificate

active

07022165

ABSTRACT:
A tubular hydrogen permeable metal membrane and fabrication process comprises obtaining a metal alloy foil having two surfaces, coating the surfaces with a metal or metal alloy catalytic layer to produce a hydrogen permeable metal membrane, sizing the membrane into a sheet with two long edges, wrapping the membrane around an elongated expandable rod with the two long edges aligned and overlapping to facilitate welding of the two together, placing the foil wrapped rod into a surrounding fixture housing with the two aligned and overlapping foil edges accessible through an elongated aperture in the surrounding fixture housing, expanding the elongated expandable rod within the surrounding fixture housing to tighten the foil about the expanded rod, welding the two long overlapping foil edges to one another generating a tubular membrane, and removing the tubular membrane from within the surrounding fixture housing and the expandable rod from with the tubular membrane.

REFERENCES:
patent: 2456163 (1948-12-01), Watson
patent: 2958391 (1960-11-01), Derosset
patent: 3350845 (1967-11-01), McKinley
patent: 3350846 (1967-11-01), Makrides et al.
patent: 3393098 (1968-07-01), Hartner et al.
patent: 3779583 (1973-12-01), Nuber
patent: 3820222 (1974-06-01), Lieberman
patent: 3957534 (1976-05-01), Linkohr et al.
patent: 4468235 (1984-08-01), Hill
patent: 4496373 (1985-01-01), Behr et al.
patent: 5139541 (1992-08-01), Edlund
patent: 5149420 (1992-09-01), Buxbaum et al.
patent: 5181941 (1993-01-01), Najjar et al.
patent: 5205841 (1993-04-01), Vaiman
patent: 5215729 (1993-06-01), Buxbaum
patent: 5217506 (1993-06-01), Edlund et al.
patent: 5259870 (1993-11-01), Edlund
patent: 5358553 (1994-10-01), Najjar et al.
patent: 5393325 (1995-02-01), Edlund
patent: 5498278 (1996-03-01), Edlund
patent: 5614001 (1997-03-01), Kosaka et al.
patent: 5644829 (1997-07-01), Mason et al.
patent: 5645626 (1997-07-01), Edlund et al.
patent: 5738708 (1998-04-01), Peachey et al.
patent: 5782960 (1998-07-01), Ogawa et al.
patent: 5888273 (1999-03-01), Buxbaum
patent: 5931987 (1999-08-01), Buxbaum
patent: 6152987 (2000-11-01), Ma et al.
patent: 6183543 (2001-02-01), Buxbuam
patent: 6214090 (2001-04-01), Dye et al.
patent: 6267801 (2001-07-01), Baake et al.
patent: 6461408 (2002-10-01), Buxbaum
patent: 2 136 362 (1999-09-01), None
Holleck, G.L. Hydrogen Diffusion through (Palladium—Silver)-Tantalum-(Palladium—Silver) Composites. J. Phys. Chem. 1970, 74 (9), 1957.
Boes, N.; Züchner, H. Diffusion of Hydrogen and Deuterium in Ta, Nb, and V. Phys. stat. sol. (a) 1973, 17, K111.
Boes, N.; Züchner, H. Application of Electrochemical Techniques for Studying Diffusion of Hydrogen Isotopes in V, Nb and Ta. Zeitschrift für Naturforschung A 1976, 31, 760.
Boes, N.; Züchner, H. Preparation of Hydrogen Permeable Foils of V, Nb and Ta by Means of Ultra High Vacuum Techniques, Zeitschrift für Naturforschung A 1976, 31, 754.
Boes, N.; Züchner, H. Secondary ion mass spectrometry and Auger electron spectroscopy investigations of Vb metal foils prepared for hydrogen permeation measurements. Surf. Tech. 178, 7, 401.chniques. Zeitschrift für Naturforschung A 1976, 31, 754.
Züchner, H. Multilayer problems in studying the diffusion of hydrogen in metals by time-lag techniques. Trans. JIM (Trans. JIM) 1980, 21 (supplement), 101.
Buxbaum, R.E. The use of Zirconium-Palladium Windows for the Separation of Tritium from the Liquid Metal Breeder-Blanket of a Fusion Reactor. Sep. Sci. Tech. 1983, 18 (12 & 13), 1251.
Hsu, C.; Buxbaum; R.E. Palladium-catalyzed oxidative diffusion for tritium extraction from breeder-blanket fluids at low concentrations. J. Nucl. Mater. 1986, 141-143, 238.
Weirich, W.; Biallas, B.; Kügler, B.; Oertel, M.; Pietsch, M.; Winkelmann, U. Development of a laboratory cycle for a thermochemical water-splitting process (Me/MeH cycle). Int. J. Hydrogen Energy 1986, 11 (7), 459.
Nishimura, C.; Komaki, M.; Amano, M. Hydrogen Permeation Characteristcs of Vanadium-Nickel Alloys. Mater. Trans., JIM 1991, 32 (5), 501.
Amano, M.; Komaki, M.; Nishimura, C. Hydrogen permeation characteristic of palladium-plated V-Ni alloy membranes. J. Less-Common met. 1991, 172-174, 727.
Katsuta, H.; McLellan, R.B.; Furukawa, K. Diffusivity and Permeability fo Hydrogen in Vanadium. Trans. JIM (Trans. JIM) 1980, 21 (supplement), 113.
Buxbaum, R.E.; Hsu, P.C. Measurement of diffusive and surface transport resistances for deuterium in palladium-coated zirconium membranes, J. Nucl. Mater. 1992, 189 (1), 183.
Buxbaum, R.E.; Marker, T.L. Hydrogen transport through non-porous membranes of palladium-coated niobium, tantalum and vanadium. J. Membr. Sci. 1993, 85, 29.
Edlund, D.J.; McCarthy, J. The relationship between intermetallic diffusion and flux decline in composite-metal membranes: implications for achieving long membrane lifetime. J. Membr. Sci. 1995, 107, 147.
Buxbaum, R.E.; Kinney, A.B. Hydrogen Transport through Tubular Membranes of Palladium-Coated Tantalum and Niobium. Ind. Eng. Chem. Res. 1996, 35, 530.
Buxbaum, R.E.; Subramanian, R.; Park, J.H.; Smith, D.L. Hydrogen transport and embrittlement for palladium coated vanadium—chromium—titanium alloys. J. Nucl. Mater. 1996, 233-237, 510.
Romanenko, O.G.; Tazhibaeva, I.L.; Shestakov, V.P.; Klepikov, A.K.; Chikhray, Y.V.; Golossanov, A.V.; Kolbasov, B.N. Hydrogen gas driven permeation through vanadium alloy VCr6Ti5. J. Nucl. Mater. 1996, 233-237, 376.
Peachey, N.M.; Dye, R.C. High temperature efforts at Los Alamos National Laboratory, DE96011306; Los Alamos National Laboratory: Los Alamos, New Mexico, US, 1995.
Peachey, N.M.; Snow, R.C.; Dye, R.C. Composite Pd/Ta metal membranes for hydrogen separation. J. Membr. Sci. 1996, 111, 123.
Moss, T.S.; Dye, R.C. Engineering materials for hydrogen separation, DE97002456; Los Alamos National Laboratory: Los Alamos, New Mexico, US, 1996.
Moss, T.S.; Dye, R.C. Composite Metal Membranes for Hydrogen Separation Applications, DE97007586; Los Alamos National Laboratory: Los Alamos, New Mexico, US, 1997.
Dye, R.C.; Birdsell, S.A.; Snow, R.C.; Moss, T.S.; Peachey, N. Advancing the Technology Base for High-Temperature Membranes, DE98000093; Los Alamos National Laboratory: Los Alamos, New Mexico, US, 1997.
Moss, T.S.; Peachey, N.M.; Snow, R.C.; Dye, R.C. Multilayer metal membranes for hydrogen separation. Int. J. Hydrogen Energy 1998, 23 (2), 99.
Tosti, S.; Bettinali, L.; Violante, V. Rolled thin Pd and Pd-Ag membranes for hydrogen separation and production. Int. J. Hydrogen Energy 2000, 25 (4), 319.
Tosti, S.; Bettinali, L.; Castelli, S.; Sarto, F.; Scaglione, S.; Violante, V. Sputtered, electroless, and rolled palladium-ceramic membranes. J. Membr. Sci. 2002, 196, 241.
Nishimura, C.; Komaki, M.; Hwang, S.; Amano, M. V—Ni alloy membranes for hydrogen purification. J. Alloys Compd. 2002, 330-332, 902.

LandOfFree

Say what you really think

Search LandOfFree.com for the USA inventors and patents. Rate them and share your experience with other people.

Rating

Tubular hydrogen permeable metal foil membrane and method of... does not yet have a rating. At this time, there are no reviews or comments for this patent.

If you have personal experience with Tubular hydrogen permeable metal foil membrane and method of..., we encourage you to share that experience with our LandOfFree.com community. Your opinion is very important and Tubular hydrogen permeable metal foil membrane and method of... will most certainly appreciate the feedback.

Rate now

     

Profile ID: LFUS-PAI-O-3611686

  Search
All data on this website is collected from public sources. Our data reflects the most accurate information available at the time of publication.