Trisbenzimidazoles useful as topoisomerase I inhibitors

Drug – bio-affecting and body treating compositions – Designated organic active ingredient containing – Having -c- – wherein x is chalcogen – bonded directly to...

Patent

Rate now

  [ 0.00 ] – not rated yet Voters 0   Comments 0

Details

514253, 514256, 514394, 5462734, 5483054, 544238, 544333, 544405, A61K 3144, C07D40114

Patent

active

058078746

ABSTRACT:
The present invention provides anti-neoplastic topoisomerase I inhibitors of the formula: ##STR1## wherein Ar is (C.sub.6 -C.sub.12)aryl or (6- to 12-membered) heteroaryl comprising 1-3 N, S or non-peroxide O, wherein N is unsubstituted or is substituted with (C.sub.1 -C.sub.4)alkyl; X is H, CN, CHO, OH, acetyl, CF.sub.3, OCH.sub.3, NO.sub.2 or NH.sub.2 ; each Y is individually H, (C.sub.1 -C.sub.4)alkyl or aralkyl; Y' is H or (C.sub.1 -C.sub.4)alkyl; n is 0 or 1; or a pharmaceutically acceptable salt therein.

REFERENCES:
patent: Re26065 (1966-07-01), Marvel et al.
patent: 2985661 (1961-05-01), Hien et al.
patent: 3449330 (1969-06-01), Guglielmetti et al.
patent: 3538097 (1970-11-01), Lowe et al.
patent: 4938949 (1990-07-01), Borch et al.
patent: 5106863 (1992-04-01), Hajos et al.
patent: 5112532 (1992-05-01), Ninomiya et al.
patent: 5126351 (1992-06-01), Luzzio et al.
patent: 5244903 (1993-09-01), Wall et al.
CA 123:198740 Sun et al. 1995.
Abdallah Cherif, et al., "N-(5,5-Diacetoxypent-l-yl)doxorubicin: A New Intensely Potent Doxorubicin Analogue", J. Med. Chem., 35, 3208-3214, (1992).
G. J. Fox, et al., "para-Bromination of Aromatic Amines: 4-Bromo-N,N-Dimethyl-3-(Trifluoromethyl)Aniline", Org. Syn., 55, 20-23, (1973).
Barbara Gatto, et al., "Identification of Topoisomerase I as the Cyctotoxic Target of the Protoberberine Alkaloid Coralyne", Cancer Res., 56, 2795-2800, (1996).
Masatomo Iwao, et al., "A Regiospecific Synthesis of Carbazones via Consecutive Palladium-Catalyzed Cross-coupling and Aryne-Mediated Cyclization", Heterocycles, 36, 1483-1488, (1993).
J. S. Kim, et al., "Influence of steric factors on topoisomerase I inhibition and cytotoxicity of bisbenzimidazoles related to Hoechst 33342", Abstract 4, 86th annual meeting of the American Association for Cancer Research, Toronto, Ontario, Canada, 2689, (1995).
J. S. Kim, et al., "Influence of steric factors on topoisomerase I inhibition and cytotoxicity of bisbenzimidazoles related to Hoechst 33342", Abstract 7, 3rd annual scientific retreat, Cancer Institute of New Jersey, Princeotn Marriot Forrestal Village, 28, (1995).
J. S. Kim, et al., "Steric factors associated with the topoisomerase I inhibition and cytotoxicity of substituted bisbenzimidazoles", Abstract 10, American Assn of Pharmaceutical Scientists, Eastern Regional Meeting, 27, (1995).
Jung Sun Kim, et al., "Structure-activity Relationships of Benzimidazoles and Related Heterocycles as Topoisomerase I Poisons", Biorganic & Med. Chem., 4, 621-630, (1996).
Jung Sun Kim, et al., "Substituted 2,5'-Bi-1H-benzimidazoles: Topoisomerase I Inhibition and Cytotoxicity", J. Med. Chem., 39, 992-998, (1996).
E. J. LaVoie, et al., "Structure-activity studies related to minor groove-binding ligands which inhibit mammalian DNA topoisomerase I", Abstract 1, 85th Annual Meeting of American Association for Cancer Research, Apr. 10-13, 1994, San Francisco, CA, 2699, (1994).
Darshan Makhey, et al., "Coralyne and Related Compounds as Mammalian Topoisomerase I and Topoisomerase II Poisons", Bioorg. & Med. Chem. Lett., 4, 781-791, (1996).
Darshan Makhey, et al., "Protoberberine Alkaloids and Related Compounds as Dual Inhibitors of Mammalian Topoisomerase I and II", Med. Chem. Res., 5, 1-12, (1994).
Sanath K. Meegalla, et al., "Synthesis and Pharmacological Evaluation of Agent Batracylin", J. Med. Chem., 37, 3434-3439, (1994).
Dan Peters, et al., "Synthesis of Various 5-Substituted Uracils", J. Heterocyclic Chem., 27, 2165-2173, (Nov. Dec. 19).
Daniel S. Pilch, et al., "Biophysical Characterization of a Cytotoxic, Topoisomerase I Poison", Abstract 8, 3rd annual Scientific Retreat, Cancer Institute of New Jersey, 3, (1995).
J. R. Piper, et al., "Synthesis and Antifolate Activity of 5-Methyl-5,10-dideaza Analogues of Aminopterin and Folic Acid and an Alternative Synthesis of 5,10-Dideazatetrahydrofolic Acid, a Potent Inhibitor of Glycinamide Ribonucleotide Formyltransferase", J. Med. Chem., 31, 2164-2169, (1988).
B. A. Porai-Koshits, et al., "Imidazole derivatives Synthesis of some polybenzimidazoles", J. GEn. Chem. USSR, 23 as related in Chemical Abstracts, vol. 48, Nov. 10, 1954, Col. 12740, 873-9, (1953).
B. A. Porai-Koshits, et al., "Imidazole derivatives. Synthesis of some polybenzimidazoles", Zhur. Obshchei Khim, 23, as related from Chemical Abstracts, vol. 48, Apr. 25, 1954, Col. 4523, 835-41, (1953).
Malvinder P. Singh, et al., "Synthesis and Sequence-Specific DNA Binding of a Topoisomerase Inhibitory Analog of Hoechst 33258 Designed for Altered Base and Sequence Recognition", Chem. Res. Toxicol., 5, 597-607, (1992).
Bathini Yadagiri, et al., "Convenient Routes to Substituted Benzimidazoles Synthetic Communications, 20(7), 955-963, (1990).
Allan Y. Chen et al., "DNA Topoisomerases: Essential Enzymes and Lethal Targets," Annu. Rev. Pharmacol. Toxicol., 34, 191-218 (1994).
Allan Y. Chen et al., "DNA minor groove-binding ligands: A different class of mammalian DNA topoisomerase I inhibitors," Proc. Natl. Acad. Sci., USA, 90, 8131-8135 (Sep. 1993).
Allan Y. Chen et al., "A New Mammalian DNA Topoisomerase I Poison Hoechst 33342: Cytoxicity and Drug Resistance in Human Cell Cultures," Cancer Research, 53, 1332-1337 (Mar. 15, 1993).
Peter D'Arpa et al., "Topoisomerase-targeting antitumor drugs," Biochimica et Biophysica Acta, 989, 163-177 (1989).
Robert C. Gallo et al., "Studies on the Antitumor Activity, Mechanism of Action, and Cell Cycle Effects of Camptothecin," Journal of the National Cancer Institute, 46, 789-795 (Apr., 1971).
Beppino C. Giovanella et al., "Complete Growth Inhibition of Human Cancer Xenografts in Nude Mice by Treatment with 20-(S)-Camptothecin," Cancer Research, 51, 3052-3055 (Jun. 1, 1991).

LandOfFree

Say what you really think

Search LandOfFree.com for the USA inventors and patents. Rate them and share your experience with other people.

Rating

Trisbenzimidazoles useful as topoisomerase I inhibitors does not yet have a rating. At this time, there are no reviews or comments for this patent.

If you have personal experience with Trisbenzimidazoles useful as topoisomerase I inhibitors, we encourage you to share that experience with our LandOfFree.com community. Your opinion is very important and Trisbenzimidazoles useful as topoisomerase I inhibitors will most certainly appreciate the feedback.

Rate now

     

Profile ID: LFUS-PAI-O-87756

  Search
All data on this website is collected from public sources. Our data reflects the most accurate information available at the time of publication.