Triethylenediamine process

Organic compounds -- part of the class 532-570 series – Organic compounds – Nitrogen attached directly or indirectly to the purine ring...

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C07D29502

Patent

active

041828640

ABSTRACT:
A process is provided for recovering substantially pure triethylenediamine in liquid tertiary amine solutions directly from the crude triethylenediamine reaction mixture without resort to a need to purify the triethylenediamine by crystallization. The process includes initially admixing a tertiary amine with a crude triethylenediamine liquid reaction product mixture. The admixture thus formed is then distilled under conditions such that the triethylenediamine and tertiary amine codistill as a substantially pure triethylenediamine solute in liquid tertiary amine solution. The collected codistillate being substantially free of reaction by-products can be used directly to catalyze urethane systems.

REFERENCES:
patent: 3080371 (1963-03-01), Spielberger et al.

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