Treatment of crude oils

Mineral oils: processes and products – Refining – Metal contaminant removal

Reexamination Certificate

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Details

C208S25100H, C208S20800M, C208S228000, C208S230000, C208S226000, C208S211000, C208S271000, C204S157150, C196S014520

Reexamination Certificate

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06955753

ABSTRACT:
A process and apparatus to extract and recover heavy metals and sulfur from crude oil or petroleum fuel products including the steps of emulsifying the crude oil with an emulsifying agent, adding a leach solution to the emulsified crude oil and leaching the emulsified crude oil at elevated temperature and pressure to give a leached emulsified crude oil. The leach solution may be acid or alkali. A proportion of the leach solution is extracted for recovering heavy metals. There can also be a microwave hydro-treating step using hydrogen gas at a temperature below 220° C. to ensure there is no quality degradation in the crude feed to produce a desulfurized crude oil and a hydrogen sulphide by-product and recovering sulfur from the hydrogen sulphide by-product.

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patent: 5985137 (1999-11-01), Ohsol et al.
patent: 6068737 (2000-05-01), De Chamorro et al.

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