Titanium and titanium hydride reticulates and method for making

Details Titanium and titanium hydride reticulates and method for making Titanium and titanium hydride reticulates and method for making

1983-07-01

1985-05-14

Niebling, John F.

Chemistry: electrical and wave energy

Apparatus

Electrolytic

75 20F, 428613, 423608, 502301, 502350, C25B 1100, C25C 702

Patent

active

045170690

ABSTRACT:
A self-supporting reticulate of titanium hydride (TiH.sub.2) is formed by slurry-coating an open cell organic synthetic resinous material, or other pore-former, and eliminating the carbon-containing components of binder and/or solvent, viscosity modifiers, thickening agents, and the like at a temperature below about 400.degree. C. In an analogous manner, an inorganic refractory material open cell substrate or other pore-former substrate may be slurry-coated and converted to a TiH.sub.2 reticulate in which the substrate is coated with TiH.sub.2 to yield a supported TiH.sub.2 reticulate. Either the self-supporting TiH.sub.2 reticulate, or the supported one, free of carbonaceous material, may be sintered to yield an essentially pure Ti (metal) reticulate which is essentially free of titanium carbide. Ti reticulates so formed are coated with Pt group metal oxides and used as anodes in chloroalkali cells.

REFERENCES:
patent: 2917384 (1959-12-01), Grandey
patent: 3214265 (1965-10-01), Fiedler
patent: 3214270 (1965-10-01), Valyl
patent: 3214287 (1965-10-01), Mosna
patent: 3218684 (1965-11-01), Spink
patent: 3224846 (1965-12-01), Fiedler et al.
patent: 3433632 (1969-03-01), Elbert
patent: 3647721 (1972-03-01), Salyer et al.
patent: 3897221 (1975-07-01), Salyer et al.
patent: 4133691 (1979-01-01), Kindt
patent: 4299682 (1982-04-01), Oda et al.

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