Chemistry of inorganic compounds – Silicon or compound thereof – Elemental silicon
Patent
1973-11-30
1976-01-20
Stern, Edward
Chemistry of inorganic compounds
Silicon or compound thereof
Elemental silicon
23273SP, 23301R, 23301SP, C01B 3302
Patent
active
039339815
ABSTRACT:
Disclosed is a method of purifying silicon by introducing the silicon into liquid tin-lead alloy at a certain temperature. The silicon goes into solution with the tin-lead alloy, after which the temperature of the liquid metal solution is reduced to a temperature low enough to cause the solution to become super-saturated with respect to silicon which then solidifies as pure material. The solid pure silicon is withdrawn from the tin-lead solution leaving substantially all of the impurities behind.
REFERENCES:
patent: 2402582 (1946-06-01), Scaff
patent: 3031403 (1962-04-01), Bennett, Jr.
patent: 3069240 (1962-12-01), Armand
patent: 3097068 (1963-07-01), Litz et al.
Book "Preparation of Single Crystals," by W. D. Lawson and S. Nielsen, 1958 Ed., p. 93, Buttersworths Scientific Publications, London.
Setty H. S. Nagaraja
Wakefield Gene Felix
Comfort James T.
Honeycutt Gary C.
Levine Harold
Stern Edward
Texas Instruments Incorporated
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