Thin film calorimeter

Thermal measuring and testing – Calorimetry

Reexamination Certificate

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Reexamination Certificate

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07399117

ABSTRACT:
A thin film calorimeter test station can be coupled to a controller in a thin film calorimeter. The thin film calorimeter can comprise a base substrate, a heat flux sensing device mounted on the base substrate, a mask having a hole with a predetermined area positionable above the heat flux sensing device, and a thickness control device for establishing a repeatable precise thickness layer of UV curable sample test material between the mask and the heat flux sensing device. The thin film calorimeter is used to determine several factors of UV curability. A double test platform test station can be provided so that tests at an active test platform and a dummy platform can be performed simultaneously using the same UV light source. Also, the base substrate can be thermally conductive and be mounted on a thermoelectric heater and cooler for controlling the temperature of the test. Furthermore, the base substrate can be mounted on a digital electronic scale whereby a quantity of UV curable sample test material can be weighed, exposed to UV light for a curing test and then a “factor of UV curability” in heat per weight, e.g. joules per gram, can be determined.

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Roper et al, Design and performance of a thin-film calorimeter for quantitative characterization of photopolymerizable systems, Review of Scientific Instruments, 76 (2005).
Publication: T. M. Roper et al., “Rapid Measurement of Photopolymerization Kinetic Behavior Using a Thin-Film Calorimeter”, published by the RadTech International trade show in Charlotte ,North Carolina, May 2-5, 2004.
Todd M. Roper, et al., “In Situ Characterization of Photopolymerizable Systems Using a Thin-Film Calorimeter,” published in Macromolecules 2005, 38, 10109-10116, and on the Web on Nov. 4, 2005.
Takashi Funatsu et al, Time-resolved electron microscopic analysis of the behavior of myosin heads on actin filaments after photolysis of caged ATP. The Journal of Cell Biology. vol. 121, Jun. 1993, p. 1056, left column paragraph 2 and right column paragraph 1.
Notification of Transmittal of International Search Report and Written Option dated Nov. 28, 2007 for PCT Application PCT/US06/61779.

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