Temperature indicating paint

Details Temperature indicating paint Temperature indicating paint

2002-08-23

2004-01-06

Fulton, Christopher W. (Department: 2859)

Compositions

Nonreactive analytical, testing, or indicating compositions

C374S162000, C252S962000

Reexamination Certificate

active

06673271

ABSTRACT:

The present invention relates to an irreversible temperature indicating paint.
Irreversible temperature indicating paint changes colour at one or more known temperatures. These colour changes of the temperature indicating paint indicate the temperature to which different parts of a component or components have been subjected. The final colour of the irreversible temperature indicating paint is dependent on both the temperature it is subjected to and the time period over which it is held at a raised temperature. The irreversible temperature indicating paint is applied to a component in a test situation and subsequently analysed to determine the temperatures to which different regions of the component reached during the test. Irreversible temperature indicating paint thus produce a temperature profile over the whole surface of a component rather than discrete points, if for example thermocouples are used.
Irreversible temperature indicating paints are applied to components, for example turbine blades, turbine vanes and combustors, of gas turbine engines and the gas turbine engine is run at the gas turbine engines normal operating conditions.
One known temperature indicating paint described in our UK patent GB1103059 comprises principally lead chromate, magnesium carbonate and silica.
Another known temperature indicating paint described in our UK patent GB2204874 comprises one or more of silver, gold, platinum, palladium, copper, nickel, chromium, titanium and silicon dispersed in 10 to 70 wt % solvent and resin.
Currently used temperature indicating paint do not provide colour changes at sufficiently high temperatures.
Accordingly the present invention seeks to provide a novel irreversible temperature indicating paint which has a plurality of colour changes in the temperature range 1050° C. to 1350° C. to provide colour changes at higher temperatures.
Accordingly the present invention provides an irreversible temperature indicating paint comprising cobalt silicate, alumino silicate, toluidine red, binder and a solvent.
Preferably the binder comprises acrylic resin and silicone resin.
Preferably the irreversible temperature indicating paint comprises 25 wt % to 50 wt % cobalt silicate, 0 wt % to 25 wt % alumino silicate, 0.5 wt % to 5 wt % toluidine red, 25 wt % to 40 wt % acrylic resin and 10 wt % to 20 wt % silicone resin excluding solvent.
Preferably the irreversible temperature indicating paint comprises 30 wt % to 50 wt % cobalt silicate, 0 wt % to 20 wt % alumino silicate, 0.5 wt % to 4 wt % toluidine red, 30 wt % to 35 wt % acrylic resin and 15 wt % to 20 wt % silicone resin excluding solvent.
More preferably the irreversible temperature indicating paint comprises 32.5 wt % to 45 wt % cobalt silicate, 5 wt % to 17.5 wt % alumino silicate, 0.5 wt % to 3 wt % toluidine red, 30 wt % to 32.5 wt % acrylic resin and 15 wt % to 17.5 wt % silicone resin excluding solvent.
The irreversible temperature indicating paint may comprise 33.8 wt % cobalt silicate, 16.9 wt % alumino silicate, 2.0 wt % toluidine red, 30.8 wt % acrylic resin and 16.5 wt % silicone resin excluding solvent.
The irreversible temperature indicating paint may comprise 44.7 wt % cobalt silicate, 6.4 wt % alumino silicate, 0.7 wt % toluidine red, 32.2 wt % acrylic resin and 16.0 wt % silicone resin excluding solvent.
Preferably the solvent comprises a mixture of propylene glycol ethers. Preferably the solvent comprises a mixture of 80% 1-methoxy-2-propanol and 20% dipropylene glycol monomethyl ether.


REFERENCES:
patent: 1777353 (1930-10-01), Davis
patent: 3445291 (1969-05-01), Stein
patent: 4925727 (1990-05-01), Brown et al.
patent: 5008136 (1991-04-01), Chamberlain
patent: 2003/0044986 (2003-03-01), Watson
patent: 2003/0044987 (2003-03-01), Watson et al.
patent: 2003/0049467 (2003-03-01), Watson et al.
patent: 2003/0049847 (2003-03-01), Watson et al.
patent: 1103059 (1968-02-01), None
patent: 2204874 (1988-11-01), None

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