Technique for preparation of fulvalenes

Details Technique for preparation of fulvalenes Technique for preparation of fulvalenes

1975-01-20

1976-03-02

Jiles, Henry R.

Chemistry of carbon compounds

Miscellaneous organic carbon compounds

C-metal

C07D33906

Patent

active

039418090

ABSTRACT:
A technique for preparing a wide range of fulvalenes by a reductive procedure is described. The procedure involves reducing an organic halide to its corresponding partially hydrogenated derivative which is reacted with fluoboric acid to yield a fluoborate. Deprotonation of the fluoborate yields the desired compound. The described technique maximizes the yield and quality of fulvalenes produced and permits the preparation of thia, selena and tellura fulvalenes.

REFERENCES:
solid State Communications, Vol. 14, 1974.
J. of the Am. Chem. Soc., Jan. 26, 1972.

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