Tantalum and niobium billets and methods of producing the same

Metal treatment – Stock – Vanadium – niobum – or tantalum base

Reexamination Certificate

Rate now

  [ 0.00 ] – not rated yet Voters 0   Comments 0

Details

C420S427000, C204S298150

Reexamination Certificate

active

07485198

ABSTRACT:
Extruded tantalum billets and niobium billets are described having a substantially uniform grain size and preferably an average grain size of about 150 microns or less and more preferably an average grain size of about 100 microns or less. The extruded billet can then be forged or processed by other conventional techniques to form end use products such as sputtering targets. A process for making the extruded tantalum billets or niobium billets is also described and involves extruding a starting billet at a sufficient temperature and for a sufficient time to at least partially recrystallize the billet and form the extruded billet of the present invention.

REFERENCES:
patent: 2950185 (1960-08-01), Hellier et al.
patent: 3497402 (1970-02-01), Douglass et al.
patent: 3767456 (1973-10-01), Glaski
patent: 3829310 (1974-08-01), Mahy
patent: 4141719 (1979-02-01), Hakko
patent: 4149876 (1979-04-01), Rerat
patent: 4684399 (1987-08-01), Bergman et al.
patent: 4844746 (1989-07-01), Hormann et al.
patent: 5234491 (1993-08-01), Chang
patent: 5242481 (1993-09-01), Kumar
patent: 5482672 (1996-01-01), Friedman et al.
patent: 6193821 (2001-02-01), Zhang
patent: 6323055 (2001-11-01), Rosenberg et al.
patent: 6331233 (2001-12-01), Turner
patent: 6348139 (2002-02-01), Shah et al.
patent: 2001/0001401 (2001-05-01), Segal
patent: 2002/0125128 (2002-09-01), Turner
patent: 62104180 (1987-05-01), None
patent: 1994-264232 (1994-09-01), None
patent: 11-080942 (1999-03-01), None
patent: 2000104164 (2000-04-01), None
patent: WO 8707650 (1987-12-01), None
patent: WO 99/61670 (1999-12-01), None
patent: WO 99/66100 (1999-12-01), None
patent: WO 00/31310 (2000-06-01), None
patent: WO 01/96620 (2001-12-01), None
Clark et al. “Influence of Transverse Rolling on the Microstructural and Textural Development of Pure Tantalum”, Metallurgical Transactions A, vol. 23A, Aug. 1992, pp. 2183-2191.
Schussler, ASM Handbook, vol. 2, 1990, Properties and Selection: Nonferrous Alloys and Secial-Purpose Materials, Pure Metals, Tantalum, pp. 1160-1163.
Lassila et al., “Mechanical Behavior of Tantalum and Tantalum-Tungsten Alloys: Texture Gradients and Macro/Micro-Response,” 14thU.S. Army Symposium on Solid Mechanics, Nov. 30, 1996 (14 pgs.).
Michaluk, “Deformation Behavior of Tantalum-Tangsten Alloys,”a Thesis submitted to the Faculty of Drexel University, Dec. 1993 (158 pgs.).
Michaluk et al., “The Effect of Oxygen, Grain Size, and Strain Rate on the Mechanical Behavior of Forged P/M Tantalum,” date unknown (pp. 195-204).
Hoge, “Influence of Strain Rate on Flow Stress of Tantalum,” Lawrence Radiation Labratory, University of California, Paper 15A.4, date unknown (pp. 996-1000).
Follansbee, “The Hopkinson Bar,” High Strain Rate Testing, date unknown (pp. 198-203).
Rudolph et al., “The Deformation of Tantalum-Niobium and Tantalum-Molybdenum Single Crystals,” Z. Metallkde., No. 58, H. 10, 1967 (pp. 708-713).
Regazzoni et al., “Influence of Strain Rate on the Flow Stress and Ductility of Copper and Tantalum at Room Temperature,” Inst. Phys. Conf. Ser. No. 70, paper presented at 3rdConf. Mech. Prop. High Rates of Strain, Oxford, 1984 (pp. 63-70).
Diaz et al., “Evidence for Slow Strain-Rate Embrittlement in Tantalum Due to Oxygen,” Scripta Metallurgica, vol. 13, 1979 (pp. 491-496).
Author unknown, “Reihenentwicklung von Orientierungsverteilungskunktionen,” date known (pp. 24-25) (in German).
Mundekis et al., “Effects of Rolling Schedule and Annealing on the High Strain Rate Behavior of Tantalum,” The Minerals, Metals & Materials Society, 1992 (pp. 77-96).
Arsenault et al., “Work-Hardening Characteristics of Ta and Ta-Base Alloys,” date unknown (pp. 283-301).
Landrum et al., “The Effects of Cold-Flowing on Tantalum Material Properties,” The Minerals, Metals & Materials Society, 1992 (pp. 59-76).
Keh et al., “Deformation Substructure in Body-Centered Cubic Metals,” Single Phase Materials, Chapter 5, date unknown (pp. 231-264).
Gourdin et al., “The Influence of Tungsten Alloying on the Mechanical Properties of Tantalum,” Journal De Physique IV, Colloque C8, vol. 4, Sep. 1994 (pp. C8-207-C8-212).
Author unknown, “Solid Solutions,” Chapter 6, date unknown (pp. 144-149).
Lassila et al., “Effects of Shock Prestrain on the Dynamic Mechanical Behavior of Tantalum,” Journal De Physique IV, Colloque C3, vol. 1, Oct. 1991 (pp. C3-19-C3-26).
Ulitchny et al., “The Effects of Interstitial Solute Additions on the Mechanical Properties of Niobium and Tantalum Single Crystals,” Journal of the Less-Common Metals, vol. 33, 1973 (pp. 105-116).
Pokross, “Tantalum Micro-Alloys,” supplied by the British Library, date unknown (pp. 297-330).
Hull et al., “Introduction to Dislocations,” 3rdEdition, 1984 (cover page & contents pages v-vii only).
Author unknown, “Mechanical Fundamentals,” Dieter Mech. Metallurgy, 3rdEd., 1986 (pp. 82-86).
Gray et al., “The High-Strain-Rate and Spallation Response of Tantalum, Ta-10W, and T-111,” The Minerals, Metals & Materials Society, 1992 (pp. 303-315).
Rajendran et al., “Effects of Strain Rate on Plastic Flow and Fracture in Pure Tantalum,” J. Mater. Shaping Technol., vol. 9, 1991 (pp. 7-20).
Cardonne et al., “Tantalum and its Alloys,” Advanced Materials & Processes, vol. 142, No. 3, Sep. 1992 (pp. 16-20).
Pokross, “Tantalum,” Metals Handbook, 10thEd., vol. 2, Properties and Selection: Nonferrous Alloys and Special-Purpose Materials, 1990 (pp. 571-574).
Raman et al., “Rapid Consolidation of Tantalum: Non Conventional Microstructure and Resultant Dynamic Mechanical Properties,” supplies by the British Library, date unknown (pp. 559-571).
Barbee et al., “Dislocation Structures in Deformed and Recovered Tantalum,” Journal of the Less-Common Metals, vol. 8, 1965 (pp. 306-319).
Fujii et al., “On the Rolling Deformation and Recrystallization of (111) [112]Single Crystals of High-Purity Tungsten, Molybdenum and Tantalum,” Journal of the Less-Common Metals, vol. 39, 1975 (pp. 161-172).
Welch et al., “Consideration of Anisotropy Parameters in Polycrystalline Metals,” Z. Metallkde, Bd. 74, H. 4, 1983 (pp. 233-237).
Arsenault, “Effects of Strain Rate and Temperature on Yield Points,” Transactions of the Metallurgical Society of AIME, vol. 230, Dec. 1964 (pp. 1570-1576).
Gray et al., “Influence of Peak Pressure and Temperature on the Structure/Property Response of Shock Loaded Ta and Ta-10W,” Metallurgical and Materials Transactions A, vol. 26A, Oct. 1995 (pp. 2555-2563).
Giannotta et al., “Ductility and Flow Rule of Tantalum at 20° C and 500° C,” Journal De Physique, Colloque C5, No. 8, Tome 46, Aug. 1985 (pp. C5-49-54).
Ferriss et al., “Deformation of Tantalum Single Crystals,”Transactions of the Metallurgical Society of AIME, vol. 224, Oct. 1962 (pp. 975-981).
Mitchell et al., “Mechanical Properties of Some Tantalum Alloys,” Canadian Journal of Physics, vol. 45, 1967 (pp. 1047-1062).
Arsenault, “An Investigation of the Mechanism of Thermally Activated Deformation in Tantalum and Tantalum-Base Alloys,” ACTA Metallurgica, vol. 14, Jul. 1966 (pp. 831-838).
Zerilli et al., “Description of Tantalum Deformation Behavior by Dislocation Mechanics Based Constitutive Relations,” J. Appl. Phys. vol. 68, No. 4, Aug. 15, 1990 (pp. 1580-1591).
Michaluk et al., “The Effects of Texture and Strain on the R-Value of Heavy Gauge Tantalum Plate,” Materials Science Forum, vol. 157-162, 1994 (pp. 1653-1662).
Spitzig et al., “Dislocation Arrangements in Tantalum Single Crystals Deformed in Tension at 373°K,” ACTA, Metallurgica, vol. 14, Oct. 1966 (pp. 1311-1323).
Hoge et al., “The Tempe

LandOfFree

Say what you really think

Search LandOfFree.com for the USA inventors and patents. Rate them and share your experience with other people.

Rating

Tantalum and niobium billets and methods of producing the same does not yet have a rating. At this time, there are no reviews or comments for this patent.

If you have personal experience with Tantalum and niobium billets and methods of producing the same, we encourage you to share that experience with our LandOfFree.com community. Your opinion is very important and Tantalum and niobium billets and methods of producing the same will most certainly appreciate the feedback.

Rate now

     

Profile ID: LFUS-PAI-O-4088553

  Search
All data on this website is collected from public sources. Our data reflects the most accurate information available at the time of publication.