Synthesis of zeolitic materials using ion-exchange resin

Chemistry of inorganic compounds – Silicon or compound thereof – Oxygen containing

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423277, 423326, 423330, 423335, 423339, 423328, 502 60, 502 62, 502 77, C01B 3328

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046801707

ABSTRACT:
Crystalline zeolites and zeolitic materials are prepared by crystallization from an aqueous mixture comprising a source of silica, optionally a source of alumina, and an ion-exchange resin preferably an anion-exchange resin. In a preferred form of the invention the anion-exchange resin is in the hydroxide form and the reaction mixture also contains a quaternary ammonium compound.

REFERENCES:
patent: 4061724 (1977-12-01), Grose et al.
patent: 4217240 (1980-08-01), Bergna
patent: 4257885 (1981-03-01), Grose et al.
patent: 4512961 (1985-04-01), Scherzer et al.
J. L. Casci and B. M. Lowe, "use of pH Measurements to Monitor Zeolite Crystallization", Zeolites, vol. 3, No. 3, Jul. 1983, pp. 186-187.
The Condensed Chemical Dictionary, Tenth Edition, Revised by Gessner G. Hawley, Von Nostrand Reinhold Co., 1981.
Kuei-Jung Chao et al, "Kinetic Studies on the Formation of ZSM-J", J. Chem. Soc., Faraday Trans. 1, 1981, 77, 547-555.

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