Synthesis of zeolite beta

Chemistry of inorganic compounds – Silicon or compound thereof – Oxygen containing

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C01B 3334

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active

051397595

ABSTRACT:
Zeolite beta is synthesized hydrothermally from an aqueous reaction mixture containing the conventional reactive sources of SiO.sub.2, Al.sub.2 O.sub.3 and Na.sub.2 O tetraethylammonium halide as the source of the crystallization directing tetraethylammonium ions and diethanolamine as the agent providing the increased basicity necessary for the formation of zeolite beta crystals. Seed crystals of zeolite beta are optionally employed to shorten the crystallization period.

REFERENCES:
patent: 3308069 (1967-03-01), Wadlinger et al.
patent: 4554145 (1985-11-01), Rubin
patent: 4642226 (1987-02-01), Calvert et al.
patent: 4923690 (1990-05-01), Valyocsik et al.

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