Synthesis of trithiocarbonate raft agents and intermediates...

Organic compounds -- part of the class 532-570 series – Organic compounds – Thiocarboxylic acids or salts thereof

Reexamination Certificate

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C423S414000, C558S243000, C558S244000, C528S196000

Reexamination Certificate

active

07632966

ABSTRACT:
This invention provides an efficient method for synthesizing trithiocarbonate RAFT agents, RSC(S)SR′, that can be used in the living polymerization of methacrylates and other olefinic monomers. This invention also provides an efficient method of synthesizing bis(alkylsulfanylthiocarbonyl) disulfides that are useful as intermediates in the synthesis of trithiocarbonate RAFT agents.

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Gareau et al. Free Radical Reaction of Diisopropyl Xanthogen Disulfide with Unsaturated Systems, 1998, Heterocycles, vol. 48, No. 10, 2008, 2016.
Thang, et al. A Novel Systhesis of Functional Dithioesters, Dithiocarbamates, Xanthates and Trithiocarbonates, Tetrahedron Letters, 1999, vol. 40, No. 13, 2436, 2437.

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