Synthesis of tetradecahydroundecaborate (-1) from borohydride io

Details Synthesis of tetradecahydroundecaborate (-1) from borohydride io Synthesis of tetradecahydroundecaborate (-1) from borohydride io

1978-07-21

1979-05-08

Peters, G. O.

Chemistry of inorganic compounds

Boron or compound thereof

Hydrogen and metal or ammonium containing

2606065B, C01B 3518

Patent

active

041536720

ABSTRACT:
The tetradecahydroundecaborate(-1) anion is synthesized from a metal borohydride by heating a suspension of the borohydride ion in a solvent, such as diglyme, with agitation at a temperature of from 85.degree. C. to about 135.degree. C. and adding an alkyl halide. The B.sub.11 H.sub.14.sup.- anion obtained is useful in the synthesis of decaborane, an intermediate in formation a carborane-based polymers.

REFERENCES:
patent: 2994718 (1961-08-01), Pearson et al.
Bell et al.; "Journ. Am. Chem. Soc."; vol. 88, p. 1473, 1966.
Brown et al.; "Jour. Am. Chem. Soc."; vol. 80, p. 1555, 1958.

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