Synthesis of S-3-chloro-1,2-propanediol

Details Synthesis of S-3-chloro-1,2-propanediol Synthesis of S-3-chloro-1,2-propanediol

1979-05-17

1982-01-26

Mars, Howard T.

Organic compounds -- part of the class 532-570 series

Organic compounds

Oxygen containing

568866, 568388, 568460, 568392, 424343, 568676, 568600, 560 30, C07C 2914, C07C 3120

Patent

active

043130089

ABSTRACT:
The S-enantiomer of 3-chloro-1,2-propanediol is prepared by reaction of a chlorodeoxy-D-saccharide having the partial structure. ##STR1## to cleave the glycol, reduce the aldehyde so formed to an alcohol, and hydrolyse the alcohol under mild acidic conditions.

REFERENCES:
Guthrie et al., Introduction to Carbohydrate Chemistry, pp. 84-86.
Whistler et al., Methods in Carbohydrate Chemistry, Academic Press, New York, 1963, vol. II, p. 67.
Pigman, The Carbohydrates, Academic Press, New York, 1957, pp. 215-219, 346-349.
Weininger, Contempory Organic Chemistry, Holt Rinehart & Winston Inc., 1972, p. 262.

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