Synthesis of refractory materials

Compositions: ceramic – Ceramic compositions – Refractory

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501 97, 501 98, 423406, C04B 3558

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active

044593635

ABSTRACT:
Refractory metal nitrides are synthesized during a self-propagating combustion process utilizing a solid source of nitrogren. For this purpose, a metal azide is employed, preferably NaN.sub.3. The azide is combusted with Mg or Ca, and a metal oxide is selected from Groups III-A, IV-A, III-B, IV-B, or a rare earth metal oxide. The mixture of azide, Ca or Mg and metal oxide is heated to the mixture's ignition temperature. At that temperature the mixture is ignited and undergoes self-sustaining combustion until the starter materials are exhausted, producing the metal nitride.

REFERENCES:
Newsline Weekly Bull., Lawrence Livermore Nat. Lab., vol. 7, No. 25, Jun. 30, 1982.
Borovinskaya et al., Poroshkovaya Metallurgica, No. 11 (191) pp. 42-45, 1978.
Merzhanov et al., Doklady Akademii Nauk USSP, vol. 204, No. 2, pp. 366-369, May 1972.
Holt, Industrial Research and Development, pp. 88-91, Apr., 1983.
Fedoroff et al., Encyc. of Explosives and Related Items pp. _A601-A619 (Picatinny Arsenal, Dover, NJ U.S.A., 1960.

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