Synthesis of pure disilicon hexafluoride

Chemistry of inorganic compounds – Silicon or compound thereof – Halogen containing

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423342, C01B 3308

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active

057119252

ABSTRACT:
Highly pure disilicon hexafluoride is synthesized by a process in which a suspension of a fluorination agent is made by dispersing this fluorination agent in an oxybenzene compound as a solvent and disilicon hexachloride is dripped in the suspension to be caused to react with the fluorination agent in nitrogen gas flows under atmospheric pressure, the oxybenzene being expressed by a following formula: ##STR1## (where each of R.sub.1 and R.sub.2 is an alkyl group alternatively having one or more substituents; carbon numbers summed up by R.sub.1 and R.sub.2 are equal to at least 2; and m.gtoreq.1 and n.gtoreq.0).

REFERENCES:
Weast, "Handbook of Chemistry & Physics", 52nd edition, 1971 (no month), pp. C-162.

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