Synthesis of nano-materials in ionic liquids

Specialized metallurgical processes – compositions for use therei – Processes – Producing or purifying free metal powder or producing or...

Reexamination Certificate

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C075S365000, C075S371000, C977S896000

Reexamination Certificate

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07547347

ABSTRACT:
A method of synthesizing nanoparticles includes: combining at least one stabilizing agent, at least one precursor and an ionic liquid to form a reaction mixture; heating the reaction mixture to a predetermined temperature to form the nanoparticles and cause the nanoparticles to self-separate from the reaction mixture; and collecting the nanoparticles from the reaction mixture. Ionic liquid from which the nanoparticles are separated may be reused.

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Ott, L.S. et al., “Nanoclusters in Ionic Liquids: Evidence for N-Heterocyclic Carbene Formation from Imidazolium-Based Ionic Liquids Detected by 2H NMR”, J. Am. Chem. Soc., vol. 127, pp. 5758-5759, published on Web Apr. 5, 2005.

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