Synthesis of molybdenum hexacarbonyl

Details Synthesis of molybdenum hexacarbonyl Synthesis of molybdenum hexacarbonyl

1987-04-20

1988-08-09

Doll, John

Chemistry of inorganic compounds

Carbon or compound thereof

Oxygen containing

423416, 423418, 423606, C01G 104, C01G 3900

Patent

active

047626992

ABSTRACT:
Molybdenum hexacarbonyl is prepared by carbonylating diammonium oxopentachloromolybdate (V) (NH.sub.4).sub.2 (MoOCl.sub.5) at pressures up to about 2000 psig and temperatures up to about 150.degree. C. in a solvent such as tetrahydrofuran, using a metallic reductant such as magnesium and an oxygen scavenger such as aluminum trichloride.

REFERENCES:
patent: 2952521 (1960-09-01), Podall
patent: 2952523 (1960-09-01), Podall
patent: 2952524 (1960-09-01), Podall
patent: 2963346 (1960-12-01), Ecke
patent: 2964387 (1960-12-01), Podall
patent: 3345144 (1967-10-01), Klopfor et al.
patent: 3810967 (1974-05-01), Arai et al.
patent: 4476103 (1984-10-01), Sapienza et al.

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