Chemistry of carbon compounds – Miscellaneous organic carbon compounds – C-metal
Patent
1977-04-11
1978-10-31
Gotts, Lewis
Chemistry of carbon compounds
Miscellaneous organic carbon compounds
C-metal
260463, C07F 1504
Patent
active
041234464
ABSTRACT:
A process is described for preparing metal alkyl carbonates, useful as carboxylating agents, which comprises reacting an inorganic metal salt with an aliphatic monohydric alcohol containing 1 to 3 carbon atoms and carbon dioxide under substantially anhydrous conditions in the presence of a solid acid acceptor, said alcohol being employed in sufficient amount to form a solution of the resulting metal alkyl carbonate in the alcohol.
REFERENCES:
patent: 3445497 (1969-05-01), Anderson et al.
patent: 4022813 (1977-05-01), Neri et al.
M. Stiles and H. Finkbeiner, JACS, 81, pp. 505-506; 2598-2599, (1969).
M. Stiles, Ann, N. Y., Acad. Sci., 88, pp. 332-340, (1970).
Fieser & Fieser, Reagents for Org. Synth., pp. 631-633, (1967).
Dow Chemical USA Applications Bulletins, "Dowex MWA-1," and Dowex Sar.
Sifniades Stylianos
Tunick Allen A.
Wohlers Herbert C.
Allied Chemical Corporation
Eakin Molly C.
Gotts Lewis
Harman Robert A.
North Robert J.
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