Synthesis of intermediate useful in the preparation of nojirimyc

Details Synthesis of intermediate useful in the preparation of nojirimyc Synthesis of intermediate useful in the preparation of nojirimyc

1988-09-16

1990-03-13

Schofer, Joseph L.

Organic compounds -- part of the class 532-570 series

Organic compounds

Carbohydrates or derivatives

536 179, 25218826, 25218827, C07H 1702

Patent

active

049084399

ABSTRACT:
5-Amino-5-deoxy-1,2-O-isopropylidene-.alpha.-D-glucofuranose is conveniently prepared by a hydride reduction of 5-azido-5-deoxy-1,2,O-isopropylidene-.alpha.-D-glucuronolactone and can readily be converted to nojirimycin, deoxynojirimycin or homonojirimycin.

REFERENCES:
patent: 4634765 (1987-01-01), Liu
B. P. Bashyal et al., Tetrahedron Letters, 27(27), 3205-3208 (1986).
B. P. Bashyal et al., Tetrahedron, 43(2), 415-422 (1987).
Y. Tsuda et al., Heterocycles, 27(1), 63-66 (1988).
Hudlicky, Milos, Reductions in Organic Chemistry, Halsted Press: New York, 1984, pp. 76, 152-154.

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