Synthesis of intermediate for the manufacture of 5,6-dihydro-2-m

Organic compounds -- part of the class 532-570 series – Organic compounds – Heterocyclic carbon compounds containing a hetero ring...

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564202, C07D32706

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active

043595790

ABSTRACT:
2-[(2-hydroxyethyl)thio]-3-oxo-N-phenylbutanamide, which is an intermediate useful in the manufacture of the fungicide, 5,6-dihydro-2-methyl-N-phenyl-1,4-oxathiin-3-carboxamide, is made by reaction of di-(2-hydroxyethyl) disulfide with acetoacetanilide in its ionized form.

REFERENCES:
patent: 3393202 (1968-07-01), Kulka et al.
patent: 3399214 (1968-08-01), Kulka et al.
patent: 3882237 (1975-05-01), Knight et al.
patent: 4230871 (1980-10-01), Lee

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