Synthesis of high purity dimethylaluminum hydride

Details Synthesis of high purity dimethylaluminum hydride Synthesis of high purity dimethylaluminum hydride

1989-01-18

1990-05-08

Shaver, Paul F.

Organic compounds -- part of the class 532-570 series

Organic compounds

Aluminum containing

C07F 506

Patent

active

049240196

ABSTRACT:
The waste product from the synthesis of trimethylgallium is reacted with a hydride selected from an alkali metal hydride, a group IIIA hydride, or a group III hydride to produce dimethylaluminum hydride of high purity.

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Lehmkuhl et al., "Metallorganische Verbindungen", (1970), p. 58, Georg Thieme Verlag, Stuttgart.
Gaines et al., "Inorganic Synthesis", 15, p. 208, pp. 203-206.
R. Bhat et al., J. of Crystal Growth, 77 (1986), pp. 7-10.
Thomas Wartik et al., Reactions of Lithium Aluminum Hydride with Representative Elements of the Main Groups of the Periodic System, Feb. 20, 1953, pp. 835-839, J.A.C.S. 75.

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