Chemistry of inorganic compounds – Zeolite – Organic compound used to form zeolite
Reexamination Certificate
2011-08-23
2011-08-23
Brunsman, David M (Department: 1732)
Chemistry of inorganic compounds
Zeolite
Organic compound used to form zeolite
C423S708000
Reexamination Certificate
active
08003074
ABSTRACT:
A process for producing ZSM-48 comprises crystallizing an aqueous reaction mixture comprising at least one source of silica, at least one source of alumina, at least one source of hydroxyl ions, at least one source of diquaternary alkylammonium, R2+, ions having the formula:in-line-formulae description="In-line Formulae" end="lead"?(CH3)3N+(CH2)5N+(CH3)3in-line-formulae description="In-line Formulae" end="tail"?and optionally ZSM-48 seed crystals, wherein said reaction mixture has a composition including the following molar ratios:R2+:SiO2less than 0.1SiO2:Al2O3less than 100OH−:SiO2less than 0.2.
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Song-Ho Lee, et al., “Reinvestigation into the synthesis of zeolites using diquaternary alkylammonium ions (CH3)3N+(CH2)nN+(CH3)3with n = 3-10 as structure-directing agents”,Microporous and Mesoporous Materials, vol. 68 (2004) 97-104.
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Elia Christine N.
Kay Robert E.
Lai Wenyih Frank
Roth Wieslaw J.
Brunsman David M
ExxonMobil Research and Engineering Company
Mareschal Ann M.
Weisberg David M.
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