Synthesis of geminal dinitro compounds

Details Synthesis of geminal dinitro compounds Synthesis of geminal dinitro compounds

1985-01-31

1986-06-10

Hollrah, Glennon H.

Organic compounds -- part of the class 532-570 series

Organic compounds

Heterocyclic carbon compounds containing a hetero ring...

549 28, 549 63, 549 88, 549346, 549424, 549481, 549510, 560156, 562553, 568589, 568704, 568712, 568926, 568944, 260688, C07D30508, C07D33342, C07C 7904, C07C 7908

Patent

active

045944300

ABSTRACT:
Geminal dinitro compounds are prepared by reacting an organic nitro compound having a replaceable hydrogen on the carbon to which the nitro group is attached with a source of nitrite ions in the presence of an oxidizing agent and a catalytic amount of an alkali metal ferricyanide.

REFERENCES:
patent: 2997504 (1961-08-01), Schecter et al.
patent: 3020319 (1962-02-01), Klager et al.
patent: 3024288 (1962-03-01), Klager
Kornblum et al, J. Org. Chem., vol. 48, No. 3, pp. 332-337, 1983; "Oxidat Substitution of Nitroparaffin Salts".
Chem. and Engineering News, vol. 39, No. 24, 6/12/61, p. 44, Reaction Gives gem-Dinitro Compounds.
Matacz et al, Chem. Abstracts, vol. 96, No. 17, #142256a, ".alpha.-Dinitro Compounds", 1981.

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